Spinsolve 90 MHz Benchtop NMR Spectrometer

The Spinsolve 90 MHz Benchtop NMR Spectrometer from Magritekdelivers unique performance at 90 MHz.

Image Credit: Magritek

Outstanding Features of Spinsolve 90 MHz

Highest sensitivity > 240:1 (For dual channel 1% ethyl benzene¹)

¹H (Proton) frequency: 90 MHz

1H and19F on all systems + X nuclei for dual channel systems

Linewidth Spinsolve 90 MHz: <0.4 Hz (50%) / <16 Hz (0.55%)

Optimized 3D pulsed field gradient for gradient-enhanced techniques

No cryogens required

Easy to use - push button acquisition

Included external hardware lock means no need for deuterated solvents to lock

Optional PFG gradients enables diffusion spectroscopy

Compatible with on-line reaction monitoring accessory

Optional automatic sample changer

Unmatched stability

Benchtop size and weight:

Weight: 115 kg (253.5 lb)

Dimensions: 66 x 45 x 43 cm (25.9″ x 17.7″ x 16.9″)

¹Sensitivity measured in a single scan on a 1% ethylbenzene sample dissolved in deuterated chloroform. The signal used for the calculation is one of the methylene group and the noise is evaluated for a signal-free region between the aromatic and the methylene signals.

Structure Confirmation with fast and powerful, advanced Multi-Nuclear Methods

Spinsolve 90 MHz Spectra Examples

2 minute HSQC-ME ofGibberellic Acidat 250 mMolar concentration acquired at 90MHz using NUS

90 MHz HSQC-ME-NUSof Gibberellic Acid at 250 mMolar. Image Credit: Magritek

90 MHz NMR spectra of Brucine at 250 mMolar concentration

Brucine 1D Proton Spectrum - 90 MHz. Image Credit: Magritek

Brucine 1D Carbon 90 MHz. Image Credit: Magritek

Brucine COSY 90 MHz. Image Credit: Magritek

2D HSQC-ME-NUS Brucine 250 mM 90 MHz. Image Credit: Magritek

Brucine Jres 90 MHz. Image Credit: Magritek

Specifications

Nuclei: ¹H, ¹⁹F, ¹³C (available with other Nuclei)

Proton Operating frequency: >90 MHz (¹H)

Nuclei: ¹H, ¹⁹F, ¹³C, ³¹P, ⁷Li, ¹¹B, ²⁹Si, ¹²⁹Xe, ²D, ¹⁵N

Resolution/LinewidthSpinsolve 90 MHz: <0.4 Hz (50%) / <16 Hz (0.55%)

Operating temperature range: 18 °C to 28 °C (65 °F to 82 °F)

¹H Sensitivity: >240:1 for 1% Ethyl Benzene (dual channel)

Uses Standard 5 mm OD NMR sample tubes, 7″ length

Minimum sample volume: 250 mL

External Hardware Lock with no requirement for deuterated solvents

3D PFG gradients maximized for gradient-enhanced techniques

Optional PFG gradients available for diffusion spectroscopy (>0.2 T/m)

Weight: 115 kg (253.5 lb)

Stray Field: <2 G all-round system

Dimensions: 66 x 45 x 43 cm (25.9″ x 17.7″ x 16.9″)

Voltage Requirement: 100 to 240 VAC, 50/60 Hz