ACQUIP, INC.
ACQUIP, INC engineers have performed numerous alignment inspections and adjustments on an extreme……...
Rapid, Benchtop NMR Analysis with the Spinsolve® Phosphorus
The Magritek Spinsolve® Phosphorus benchtop NMR spectrometer can help users obtain a remarkable level of spectroscopic detail.
31P is a completely natural nucleus that exists abundantly in many organic compounds. The high NMR sensitivity, simple spectra and large chemical shift range of 31P and the lack of common background signals (such as solvent signals) make 31P NMR suitable for routine purity assessment and reaction monitoring.
Key Features and Benefits
Compact and convenient
Easy to operate
High Performance
Low Maintenance
Applications
Purity analysis of organic compounds
Reaction monitoring
Pharmaceutical analysis
Structure elucidation
Download the Brochure for More Information
Assaying Sample Purity
The highly sensitive Spinsolve® benchtop spectrometer in combination with the simple phosphorus spectrum makes Spinsolve® Phosphorus suitable for purity assays.
Reaction Monitoring
It takes 5h for oxidation of triphenylphosphine into triphenylphosphine sulfide. Monitoring the reaction is simple due to the clean separation and minimum number of peaks in the spectrum.
Pulse Sequences Available on the Spinsolve Phosphorus
| Proton | Fluorine | Phosphorus |
|---|---|---|
| 1DParamagnetic2D COSY2D JREST1, T2Reaction Monitoring | 1DParamagnetic2D F- COSY2D F – JRES2D FH – COSYReaction Monitoring | 1DNOE (on/off)Proton decoupling (on/off)Reaction Monitoring |
Specifications
| Spinsolve Phosphorus Specifications | |
|---|---|
| Nuclei | 1H, 19F, 31P |
| Operating frequency | 43 MHz (1H) |
| 1H 50% linewidth | < 0.5 Hz |
| 1H 0.55% linewidth | <20 Hz |
| 1H sensitivity | > 70:1 for 1% Ethyl Benzene |
| Operating temperature range | 20° C to 25° C (68°F to 78°F) |
| Dimensions | 58 X 43 X 40 cm (23” x 17” x16”) |
| Weight | 55 kg (120 lbs) |
| Stray field | < 2 G all around system |
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