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PolyBLOCK 8: A Compact 8 Reactor, Bench-Top, Automated Parallel Synthesis Platform
The PolyBLOCK 8 is a highly versatile, compact 8-reactor, automated parallel synthesis platform, perfect for use in general chemical synthesis within the R&D and process development fields, whilst also proving effective for more bespoke applications, such as long-term stability studies. The 8independently controlled reaction zones make the PolyBLOCK 8 especially well-suited for DoE campaigns and the platform’s modular design enables its capabilities to be easily expanded and adapted
Application modules that can be added include:
It supports reactor volumes of up to 150 ml, and is equipped with adaptors to support a range of reactor types and sizes. Additional functionality modules include:
The system is also available in a high-pressure variant.
Features and Options:
Temperature Control
Ambient to 250 ⁰C (without external cooling)
Options to decrease the range down to-40 ⁰C(circulator dependent)
Separate mantle around each reactor allows the temperature to be controlled individually, with arange/difference of over 50 °C between the reactors
Independent Stirring
Indirect agitation with magnetic stirrer bar as standard.
- Suspended mechanical agitation for efficient mixing on small-scale and non-viscous samples.
- Optional Overhead direct agitation for larger vessels.
Intelligent Software Control and Analysis
labCONSOL software control enables regular data logging, multi-step recipes, parameter control, and feedback loops. The software adds a responsive intelligence to the PolyBLOCK 4 system and still delivers an intuitive interface that needs only minimal training to run quickly.
Safety Features
Include automatic user-configurable reaction detection and shutdown procedures,to ensure user safety.
Automatic hardware and software fail-safes are installed on every system.
Condensing Options
- Easy quick-connect solution for condensing and inerting in larger reactors. Seals allow condensers to be removed without cooling liquid spillage.
Also available reflux and inerting block, with adapters for vials, tubes, and reactors.
Reactor Options
Vessel typesare available in Glass, Stainless Steel orHastelloy. With reactor volumes up to 150 ml.
High Pressure and Vacuum Systemsavailable, more details on our high-pressure system can be found via PolyBLOCK High Pressure.
Sampling Systemsthrough active pumps, manual dip tubes, automated level control, or multisampling units, like the ASU.
Reagent Additionthrough fully automated liquidand gas feeds as well as volumetric syringe pumps. These solutions can be applied to both high and low-pressure systems.
Control Optionsall relevant inputs can be logged, enabling automated monitoring and, where appropriate, feedback control of the reactor system.
Sensor Options
Temperature, pressure, pH, turbidity, conductivity.
Integration of third-party probes is possible, such as in-situ FTIR, particle sizing probes and Raman probes.
- Suspended mechanical agitation for efficient mixing on small-scale and non-viscous samples.
- Optional Overhead direct agitation for larger vessels.
Intelligent Software Control and Analysis
- Easy quick-connect solution for condensing and inerting in larger reactors. Seals allow condensers to be removed without cooling liquid spillage.
Also available reflux and inerting block, with adapters for vials, tubes, and reactors.
Reactor Options
Vessel typesare available in Glass, Stainless Steel orHastelloy. With reactor volumes up to 150 ml.
High Pressure and Vacuum Systemsavailable, more details on our high-pressure system can be found via PolyBLOCK High Pressure.
Sampling Systemsthrough active pumps, manual dip tubes, automated level control, or multisampling units, like the ASU.
Reagent Additionthrough fully automated liquidand gas feeds as well as volumetric syringe pumps. These solutions can be applied to both high and low-pressure systems.
Control Optionsall relevant inputs can be logged, enabling automated monitoring and, where appropriate, feedback control of the reactor system.
Sensor Options
Temperature, pressure, pH, turbidity, conductivity.
Integration of third-party probes is possible, such as in-situ FTIR, particle sizing probes and Raman probes.
labCONSOL software control enables regular data logging, multi-step recipes, parameter control, and feedback loops. The software adds a responsive intelligence to the PolyBLOCK 4 system and still delivers an intuitive interface that needs only minimal training to run quickly.
Safety Features
Include automatic user-configurable reaction detection and shutdown procedures,to ensure user safety.
Automatic hardware and software fail-safes are installed on every system.
Condensing Options
- Easy quick-connect solution for condensing and inerting in larger reactors. Seals allow condensers to be removed without cooling liquid spillage.
Ambient to 250 ⁰C (without external cooling)
Options to decrease the range down to-40 ⁰C(circulator dependent)
Separate mantle around each reactor allows the temperature to be controlled individually, with arange/difference of over 50 °C between the reactors
Independent Stirring
Indirect agitation with magnetic stirrer bar as standard.
Indirect agitation with magnetic stirrer bar as standard.
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