AutoMATE 8: A Linear 8 Reactor, Bench-Top, Automated Parallel Synthesis Platform

上海仪舶实验室自动化 25-01-23 14:46:37

AutoMATE 8: A Linear 8 Reactor, Bench-Top, Automated Parallel Synthesis Platform

The AutoMATE 8 is a linear and versatile, 8-reactor, automated parallel synthesis platform, perfect for usage in general chemical synthesis within R&D and process development, along with other more specific and bespoke applications.As with the PolyBLOCK 8, the eight independently controlled reaction zones make AutoMATE 8 especially well-suited for DoE campaigns and the platform’s modular design allows for a huge variety and range of applications.In particular, the linear reactor design of the AutoMATE 8 makes it ideal for more demanding applications, such as thosewhere numerousinputs and outputs are required.

Application modules that can be added include:

  • Solubility/crystallization monitoring

  • Online calorimetry option

  • Catalyst screening

    It supports reactor volumes of up to 150ml per reactor, and is equipped with adaptors to support a range of reactor types and sizes. Additional functionality modules include:

  • Liquid dosing

  • Gas feed

  • Liquid sampling, including integration with the ASU

  • Quick-connect refluxing option

  • Quick-connect inerting solution

  • pH monitoring

    Features and Options:

    Temperature Control

      Ambient to 250 ⁰C (without external cooling).

      Options to increase the range from -40 ⁰C (circulator dependent) or up to 350 ⁰C.

      A separate mantle around each reactor allows the temperature to be controlled individually.

      With arange/difference of over 100 °C between the reactors.

      Independent Stirring

        Indirect agitation with suspended magnetic stirringas standard.

      • Suspended agitation for efficient mixing on small-scale and non-viscous samples.

      • The more spacious 'suspended'stirrers are suitablefor slurries.

      • Optional Overhead direct agitation for larger vessels.

        Intelligent Software Control and Analysis

          labCONSOL software control enables regular data logging, multi-step recipes, parameter control, and feedback loops. The software adds a responsive intelligence to the AutoMATE 8system and still delivers an intuitive interface that needs only minimal training to run quickly.

          Safety Features

            Include automatic user-configurable reaction detection and shutdown procedures, to ensure user safety.

            Automatic hardware and software fail-safes are installed on every system.

            Condenser options

            • Easy quick-connect solution for condensing and inerting in larger reactors. Seals allow condensers to be removed without cooling liquid spillage.

              Also available reflux and inerting block, with adapters for vials, tubes, and reactors

              Reactor Options

                Vessel typesare available in Glass, Stainless Steel orHastelloy. With reactor volumes up to 150ml.

                High Pressure and Vacuum Systemsavailable, more details on our high-pressure system can be found on thehigh-pressure variant.

                Sampling Systemsthrough active pumps, manual dip tubes, automated level control, or multisampling units, like theASU.

                Reagent Additionthrough fully automated liquidand gas feeds as well as volumetric syringe pumps. These solutions can be applied to both high and low-pressure systems.

                Control Optionsall relevant inputs can be logged, enabling automated monitoring and, where appropriate, feedback control of the reactor system.

                Sensor Options

                Temperature, pressure, pH, turbidity, conductivity.

                Integration of third-party probes is possible, such as in-situ FTIR, particle sizing probes and Raman probes.

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